Synthesis, characterization, and thermal decomposition of fluorinated salicylaldehyde Schiff base derivatives (salen) and their complexes with copper(II)

Mustafa Kemal Yılmaz; Göktürk Avşar

doi:10.1007/s10973-009-0453-1

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Yazarlar	Mustafa Kemal Yılmaz Göktürk Avşar
Kurum Dışı Yazarlar	Hüseyin Altınel Bilgehan Güzel
Tek Biçim Adres (URI)	https://hdl.handle.net/20.500.14114/9932
Yayın Türü	Makale
Yayın Yılı	2009
DOI Adresi	10.1007/s10973-009-0453-1
Yayıncı	Springer
Dergi Adı	Journal of Thermal Analysis and Calorimetry
Konu Başlıkları	Homojen katalizörler
İndekslenen Platformlar	Springer

Trifluoromethoxy functionalized copper(II)
Schiff base complexes N,N0
-bis(5-trifluoromethoxysalicylaldehyde)cyclohexanediiminatodiaquacopper(II) and N,N0
-
bis(5-trifluoromethoxysalicylaldehyde)phenylenediiminatocopper(II) were synthesized and characterized. Thermal
decompositions of the synthesized complexes were studied
by thermogravimetry in order to evaluate their thermal
stability and thermal decomposition pathways. Three similar decomposition steps occurred for the two copper
complexes. Mass losses and evolved gasses were characterized by
TG/DTA-MS. Kinetic parameters were calculated and the
results showed that the values obtained are comparable.

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Eser Adı dc.title	Synthesis, characterization, and thermal decomposition of fluorinated salicylaldehyde Schiff base derivatives (salen) and their complexes with copper(II)
Yazarlar dc.contributor.author	Mustafa Kemal Yılmaz
Yazarlar dc.contributor.author	Göktürk Avşar
Kurum Dışı Yazarlar dc.contributor.other	Hüseyin Altınel
Kurum Dışı Yazarlar dc.contributor.other	Bilgehan Güzel
Yayıncı dc.publisher	Springer
Yayın Türü dc.type	Makale
Özet dc.description.abstract	Trifluoromethoxy functionalized copper(II) Schiff base complexes N,N0 -bis(5-trifluoromethoxysalicylaldehyde)cyclohexanediiminatodiaquacopper(II) and N,N0 - bis(5-trifluoromethoxysalicylaldehyde)phenylenediiminatocopper(II) were synthesized and characterized. Thermal decompositions of the synthesized complexes were studied by thermogravimetry in order to evaluate their thermal stability and thermal decomposition pathways. Three similar decomposition steps occurred for the two copper complexes. Mass losses and evolved gasses were characterized by TG/DTA-MS. Kinetic parameters were calculated and the results showed that the values obtained are comparable.
Kayıt Giriş Tarihi dc.date.accessioned	2026-02-12
Yayın Yılı dc.date.issued	2009
Açık Erișim Tarihi dc.date.available	2009-09-11
Dil dc.language.iso	eng
Konu Başlıkları dc.subject	Homojen katalizörler
Atıf İçin Künye dc.identifier.citation	J Therm Anal Calorim (2010) 101:199–203
Haklar dc.rights	Journal of Thermal Analysis and Calorimetry
ISSN dc.identifier.issn	1588-2926
Sponsor Yayıncı dc.description.sponsorship	-
İlk Sayfa dc.identifier.startpage	199
Son Sayfa dc.identifier.endpage	203
Makale Numarası dc.identifier.articlenumber	-
Dergi Adı dc.relation.journal	Journal of Thermal Analysis and Calorimetry
Dergi Sayısı dc.identifier.issue	101
Dergi Cilt dc.identifier.volume	101
Tek Biçim Adres (URI) dc.identifier.uri	file:///C:/Users/Huawei/Downloads/s10973-009-0453-1.pdf
Tek Biçim Adres (URI) dc.identifier.uri	https://hdl.handle.net/20.500.14114/9932
DOI Numarası dc.identifier.doi	10.1007/s10973-009-0453-1
İndekslenen Platformlar dc.source.database	Springer

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